{"id":18213,"date":"2022-02-09T10:01:07","date_gmt":"2022-02-09T02:01:07","guid":{"rendered":"https:\/\/www.paiqinano.com\/?p=18213"},"modified":"2022-01-20T13:51:03","modified_gmt":"2022-01-20T05:51:03","slug":"%e6%b5%85%e8%b0%88-%e6%b0%9f%e7%a2%b3-%e7%9f%b3%e5%a2%a8%e7%83%af%e5%a4%8d%e5%90%88%e6%b6%82%e5%b1%82%e7%9a%84%e8%80%90%e8%85%90%e8%9a%80%e6%80%a7%e8%83%bd%e7%a0%94%e7%a9%b6%e5%8f%91%e5%b1%95%e8%bf%9b","status":"publish","type":"post","link":"https:\/\/www.paiqinano.com\/?p=18213","title":{"rendered":"\u6d45\u8c08 \u6c1f\u78b3\/\u77f3\u58a8\u70ef\u590d\u5408\u6d82\u5c42\u7684\u8010\u8150\u8680\u6027\u80fd\u7814\u7a76\u53d1\u5c55\u8fdb\u5c55"},"content":{"rendered":"
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\u521b\u4f5c\u8005\uff1a\u6234\u4eae\uff0c\u6797\u5fd7\u5cf0\uff0c\u6731\u5174\u5143\uff0c\u8bb8\u7acb\u5764<\/strong><\/p>\n

\u6765\u6e90\u4e8e\uff1a\u6b66\u6c49\u5de5\u7a0b\u5927\u5b66\uff0c\u4e2d\u56fd\u8239\u8236\u91cd\u5de5\u96c6\u56e2\u516c\u53f8\u7b2c\u4e03\u4e8c\u4e94\u7814\u7a76\u5ba4<\/strong><\/p>\n<\/section>\n<\/section>\n<\/section>\n

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\u524d\u8a00<\/strong><\/section>\n<\/section>\n<\/section>\n<\/section>\n

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\u6df1\u6d77\u7684\u4e25\u9177\u81ea\u7136\u73af\u5883\u5e38\u9020\u6210\u8239\u53ea\u3001\u6df1\u6d77\u670d\u52a1\u5e73\u53f0\u91d1\u5c5e\u6750\u6599\u96f6\u90e8\u4ef6\u6d78\u8680\uff0c\u5bfc\u81f4\u5f88\u5927\u7684\u5b89\u5168\u98ce\u9669\u3002\u6709\u673a\u6d82\u5c42\u662f\u7535\u5316\u5b66\u8150\u8680\u5b89\u5168\u9632\u62a4\u7684\u4e3b\u8981\u65b9\u5f0f\u4e4b\u4e00\uff0c\u5176\u5177\u5907\u5de5\u7a0b\u65bd\u5de5\u4fbf\u6377\u3001\u4f4e\u6210\u672c\u548c\u7ef4\u62a4\u4fdd\u517b\u7b80\u6613\u7b49\u7279\u6027\u3002<\/p>\n

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\n

\u5e38\u89c1\u7684\u6539\u6027\u6750\u6599\u65b9\u5f0f\u6709\u7269\u7406\u6539\u6027\u6750\u6599\u3001\u7269\u7406\u5b66\u5171\u6df7\u6539\u6027\u6750\u6599\u548c\u586b\u5145\u6599\u6539\u6027\u6750\u6599\uff0c\u5728\u5176\u4e2d\u586b\u5145\u6599\u6539\u6027\u6750\u6599\u4e2d\u4f7f\u7528\u7684\u989c\u586b\u5145\u6599\u53ef\u4ee5\u5177\u6709\u88c5\u9970\u548c\u63d0\u9ad8\u9540\u5c42\u7279\u6027\u7684\u529f\u6548\u3002\u4f34\u968f\u7740\u7eb3\u7c73\u590d\u5408\u6750\u6599\u5236\u53d6\u6280\u672f\u6027\u7684\u5b8c\u5584\uff0c\u7eb3\u7c73\u6280\u672f\u586b\u5145\u6599\u5728\u9540\u5c42\u4e2d\u4e5f\u83b7\u5f97\u4e86\u666e\u904d\u7684\u63a2\u8ba8\u548c\u8fd0\u7528\u3002\u8bd5\u9a8c\u53d1\u89c9\uff0c\u56e0\u4e3a\u91d1\u7eb3\u7c73\u9897\u7c92\u7269\u7406\u5b66\u89c4\u683c\u5c0f\uff0c\u6bd4\u8868\u9762\u5927\uff0c\u5bf9\u6d82\u819c\u7684\u5f3a\u5ea6\u3001\u8010\u78e8\u6027\u80fd\u3001\u9632\u7d2b\u5916\u5149\u548c\u8010\u8150\u8680\u7b49\u7279\u6027\u5177\u5907\u7edd\u4f73\u7684\u63d0\u9ad8\u5b9e\u9645\u6548\u679c\u3002<\/p>\n

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\u77f3\u58a8\u70ef\u662f\u4e00\u79cd\u4e8c\u7ef4\u7eb3\u7c73\u6280\u672f\u6784\u9020\u65b0\u578b\u6750\u6599\uff0c\u5728\u70ed\u529b\u5b66\u3001\u7535\u529b\u5b66\u3001\u7535\u5b50\u5149\u5b66\u548c\u7ed3\u6784\u529b\u5b66\u7b49\u9886\u57df\u4e3b\u8981\u8868\u73b0\u7a81\u663e\u3002\u7814\u7a76\u8868\u660e\u77f3\u58a8\u70ef\u53ef\u5408\u7406\u5730\u6539\u8fdb\u805a\u6c28\u916f\u6750\u6599\u3001\u73af\u6c27\u6811\u8102\u80f6\u3001\u4e19\u70ef\u9178\u4e73\u6db2\u7b49\u6750\u8d28\u7684\u7279\u6027\u3002\u8fd9\u662f\u7531\u4e8e\u5efa\u7b51\u6d82\u6599\u4e2d\u7684\u77f3\u58a8\u70ef\u4ee5\u5c42\u5757\u72b6\u5b58\u6709\uff0c\u5e76\u5408\u7406\u5730\u5c01\u5835\u9540\u5c42\u5b54\u9699\u5ea6\uff0c\u5bf9H2O\u3001O2\u548cCl-\u7b49\u6d78\u8680\u7269\u8d28\u5747\u8868\u660e\u51fa\u826f\u597d\u7684\u9694\u7edd\u7279\u6027\uff0c\u4e0e\u6b64\u540c\u65f6\u53ef\u4ee5\u63d0\u5347\u6d82\u819c\u7684\u8010\u8150\u8680\u6027\u548c\u878d\u5408\u6297\u538b\u5f3a\u5ea6\u3002\u77f3\u58a8\u70ef\u7684\u5206\u6563\u5316\u5bf9\u9540\u5c42\u7279\u6027\u5177\u5907\u5173\u952e\u7684\u5371\u5bb3\uff0c\u5e38\u89c1\u7684\u5206\u6563\u5316\u65b9\u6cd5\u6709\u539f\u70b9\u6c47\u805a\u3001\u6709\u673a\u5316\u5b66\u6539\u6027\u6750\u6599\u3001\u8d85\u58f0\u6ce2\u5206\u6563\u5316\u7b49\u3002\u6587\u4e2d\u6839\u636e\u8d85\u58f0\u6ce2\u5206\u6563\u5316\u7684\u65b9\u6cd5\uff0c\u8fd0\u7528\u8d85\u58f0\u6ce2\u7a7a\u5316\u6548\u5e94\u6240\u5f62\u6210\u7684\u673a\u68b0\u8bbe\u5907\u526a\u5207\u5e94\u529b\u5c06\u77f3\u58a8\u70ef\u5206\u6563\u5316\u5728\u6c1f\u78b3\u6811\u8102\u4e2d\u5236\u53d6\u590d\u5408\u578b\u9540\u5c42\u3002\u6839\u636e\u7ea2\u5916\u5149\u8c31\u53ca\u5176\u573a\u53d1\u9001\u7535\u955c\u5bf9\u77f3\u58a8\u70ef\u548c\u590d\u5408\u578b\u9540\u5c42\u7684\u5916\u90e8\u7ecf\u6d4e\u5916\u8c8c\u5f00\u5c55\u8868\u73b0\uff0c\u5bf9\u6d82\u819c\u7684\u878d\u5408\u6297\u538b\u5f3a\u5ea6\u548c\u8868\u9762\u5f20\u529b\u5f00\u5c55\u68c0\u6d4b\uff0c\u5e76\u9009\u7528\u7535\u5316\u5b66\u963b\u6297\u8c31\u548c\u76d0\u96fe\u8bd5\u9a8c\u79d1\u5b66\u7814\u7a76\u77f3\u58a8\u70ef\u5bf9\u9540\u5c42\u6297\u6c27\u5316\u7279\u6027\u7684\u5371\u5bb3\u3002<\/p>\n

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1 \u8bd5\u9a8c\u4e00\u90e8\u5206<\/strong><\/section>\n<\/section>\n<\/section>\n<\/section>\n

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1.1 \u8bd5\u9a8c\u539f\u6750\u6599\u53ca\u9884\u5907\u5904\u7406<\/strong><\/p>\n

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\u8bd5\u9a8c\u5e38\u7528\u6c1f\u78b3\u6811\u8102\u8d2d\u81ea\u5e38\u5dde\u5e02\u5609\u7f8e\u5efa\u7b51\u6d82\u6599\u6709\u9650\u8d23\u4efb\u516c\u53f8\uff1b\u77f3\u58a8\u70ef\uff08\u8584\u539a0.8~1.2 nm\uff0c\u76f4\u5f910.5~2 \u03bcm\uff0c\u5355\u9762\u7387\u7ea680%\uff09\u7531\u5357\u4eac\u5e02\u5148\u4e30\u7eb3\u7c73\u539f\u6750\u6599\u8d38\u6613\u6709\u9650\u516c\u53f8\u7ed9\u4e88\uff1bN\uff0cN-\u4e8c\u7532\u57fa\u7532\u9170\u80fa\uff08DMF\uff09\u8d2d\u81ea\u56fd\u836f\u63a7\u80a1\u5316\u5b66\u836f\u54c1\u6709\u9650\u8d23\u4efb\u516c\u53f8\uff1b\u9540\u5c42\u57fa\u6750\u539f\u6750\u6599\u4e3aQ235 \u9ad8\u78b3\u94a2\uff08C\uff1a0.15%~0.20%\uff1bMn\uff1a0.30%~0.65%\uff1bSi\u22640.30%\uff1bS\u22640.15%\uff1bP\u22640.04%\uff09\u3002\u5c06\u8bd5\u4ef6\u5207\u6210\u4e0d\u4e00\u6837\u89c4\u683c\u6837\u5b50\uff0c\u7528SiC\u6253\u78e8\u7802\u7eb8\u4ece100#\u6253\u78e8\u629b\u5149\u81f3400#\uff0c\u5404\u81ea\u7528\u7532\u82ef\u3001\u4e59\u9178\u4e59\u916f\u548c\u7eaf\u51c0\u6c34\u8d85\u58f0\u6e05\u6d17\uff0c\u70d8\u5e72\u540e\u653e\u7f6e\u5e72\u8e81\u76bf\u4e2d\u9884\u7559\u3002<\/p>\n

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1.2 \u9540\u5c42\u7684\u5236\u53d6<\/strong><\/p>\n

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\u7528\u4f53\u7ec6\u80de\u7c89\u788e\u4eeaVCX800\uff08SONICS & MATERI-ALS\uff0cINC.\uff09\u6839\u636e\u8d85\u58f0\u6ce2\u529f\u6548\u5c06\u77f3\u58a8\u70ef\uff08G\uff09\u5728\u6c1f\u78b3\u55b7\u6d82\uff08FT\uff09\u73af\u6c27\u6811\u8102\u4e2d\u5206\u6563\u5316\uff0c\u83b7\u5f97\u6df7\u548c\u5300\u79f0\u7684\u6709\u673a\u5316\u5b66\u5efa\u7b51\u6d82\u6599\uff08\u77f3\u58a8\u70ef\u7684\u6210\u5206\u5404\u81ea\u4e3a0.01wt%\u30010.05wt%\u548c0.15wt%\uff0c\u5404\u81ea\u8bb0\u4f5cFT-G1\u3001FT-G5 \u53ca\u5176FT-G15\uff09\uff0c\u6dfb\u52a0\u73af\u6c27\u56fa\u5316\u5242\u548c\u6cb9\u6f06\u7a00\u91ca\u5242\u6405\u62cc\u5747\u5300\u540e\uff0c\u9759\u653e\u719f\u62105 min\u3002\u9009\u7528\u65cb\u6d82\u7684\u65b9\u6cd5\u5728Q235\u8bd5\u4ef6\u8868\u5c42\u5236\u53d6\u6c1f\u78b3\u55b7\u6d82\/\u77f3\u58a8\u70ef\u590d\u5408\u578b\u9540\u5c42\uff08FTG\uff09\uff0c\u4e8e60 \u2103\u4e0b\u5e72\u56fa24 h\uff0c\u83b7\u5f97\u8584\u539a25\u00b13 \u03bcm\u9540\u5c42\u9884\u7559\uff0c\u6bcf\u4e00\u7ec4\u9009\u7528\u4e09\u4e2a\u5e73\u884c\u9762\u6837\u5f00\u5c55\u8bd5\u9a8c\u3002<\/p>\n

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1.3 \u5916\u90e8\u7ecf\u6d4e\u5256\u6790\u548c\u529f\u80fd\u6d4b\u8bd5<\/strong><\/p>\n

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1.3.1 \u5916\u90e8\u7ecf\u6d4e\u5256\u6790<\/strong><\/p>\n

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\u9009\u7528\u5085\u7acb\u53f6\u5149\u8c31\u5206\u6790\u4eea\uff08Thermo Sceientific Ni-colet iS10 spectrometer\uff0cThermo Fisher Scientific Inc.\uff09\u5bf9\u8bd5\u54c1\u5f00\u5c55\u5b98\u80fd\u56e2\u5f02\u6784\u68c0\u6d4b\u5206\u6790\uff0c\u626b\u63cf\u4eea\u8303\u7574\u4e3a600 ~4000 cm-1\uff0c\u7c89\u672b\u72b6\u8bd5\u4ef6\u9009\u7528KBr\u7247\u5242\u6cd5\u5236\u53d6\uff0c\u8bd5\u9a8c\u524d\u9700\u5c06\u7c89\u672b\u72b6\u572860 \u2103\u70d8\u5e72\u7bb1\u4e2d\u5e72\u8e8124 h\uff0c\u78be\u78e8\u540e\u6839\u636e\u7c89\u672b\u538b\u7247\u673a\u5236\u53d6\u73af\u5883\u8bd5\u54c1\u5e76\u68c0\u6d4b\uff0c\u5c06\u5c0f\u91cf\u7c89\u672b\u72b6\u8bd5\u4ef6\u4e0eKBr\u6df7\u548c\u78be\u78e8\uff0c\u6291\u5236\u8bd5\u9a8c\u8bd5\u54c1\u5e76\u68c0\u6d4b\uff0c\u68c0\u6d4b\u7a0b\u5e8f\u5c06\u81ea\u52d5\u6263\u51cf\u73af\u5883\u7ea2\u5916\u7ebf\u56fe\u666e\uff1b\u5c06G\u5206\u6563\u5316\u5728DMF\u4e4b\u540e\u771f\u7a7a\u5e72\u71e5\u673a\uff0c\u9009\u7528ZEISS ULTRA 55\u573a\u53d1\u9001\u626b\u63cf\u4eea\u900f\u5c04\u7535\u955c\uff08FESEM\uff09\u5bf9G\u548c\u9540\u5c42\u8868\u5c42\u5916\u90e8\u7ecf\u6d4e\u5916\u8c8c\u5f00\u5c55\u8868\u73b0\u5256\u6790\u3002<\/p>\n

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1.3.2 \u673a\u68b0\u6027\u80fd\u68c0\u6d4b
<\/strong><\/p>\n

\n

\u4f9d\u636e\u89c4\u8303ASTM D4541-2009\u300a\u7528\u4fbf\u643a\u5f0f\u9644\u7740\u529b\u6d4b\u8bd5\u4eea\u6d4b\u5b9a\u6d82\u5c42\u62c9\u8131\u5f3a\u5ea6\u300b\uff0c\u9009\u7528\u4fbf\u643a\u5f0f\u62c9\u62e8\u5f0f\u9644\u7740\u529b\u6d4b\u8bd5\u4eea\uff08ProsiTest AT\uff09\u5c06\u9540\u5c42\u4ece\u57fa\u6750\u8868\u5c42\u5206\u79bb\u51fa\u6765\uff0c\u4ee5\u68c0\u9a8c\u9540\u5c42\u4e0e\u5408\u91d1\u57fa\u6750\u95f4\u7684\u878d\u5408\u6297\u538b\u5f3a\u5ea6\uff0c\u8bd5\u4ef6\u89c4\u683c\u4e3a\u03a625 mm\u00d73 mm\u3002\u9009\u7528\u9759\u6001\u6570\u636e\u63a5\u89e6\u89d2\u6d4b\u91cf\u4eeaDSA100\uff08\u6cd5\u56fd\u514b\u9c81\u58eb\u4f01\u4e1a\uff09\u7cbe\u786e\u6d4b\u91cf\u9540\u5c42\u7684\u6c34\u8868\u9762\u5f20\u529b\uff0c\u4f9d\u636e\u89e6\u78b0\u89d2\u7684\u5927\u5c0f\u5256\u6790\u9540\u5c42\u7684\u758f\u6c34\u6027\u3002<\/p>\n

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1.3.3 \u8010\u8150\u8680\u6027\u80fd\u68c0\u6d4b
<\/strong><\/p>\n

\n

\u4f9d\u636e\u884c\u4e1a\u6807\u51c6GB\/T 1771\u20142007 \u5f00\u5c55\u76d0\u96fe\u8bd5\u9a8c\uff0c\u5c06\u8bd5\u4ef6\u6fc0\u5149\u5207\u5272\u4e3a30 mm\u00d730 mm\u00d73 mm\u5c3a\u5bf8\uff0c\u9540\u5c42\u4e4b\u5916\u4e00\u90e8\u5206\u7528\u73af\u6c27\u6811\u8102\u817b\u5b50\u7c89\u5bc6\u5c01\u6027\uff0c\u55b7\u96fe\u5668\u9971\u548c\u6eb6\u6db2\u4e3a5wt%NaCl\u9971\u548c\u6eb6\u6db2\uff0c\u8bd5\u9a8c\u7bb1\u6eab\u5ea6\u4e3a35 \u2103\u3002\u8bd5\u4ef6\u5206\u6210\u522e\u75d5\u548c\u8be6\u7ec6\u9540\u5c42\u4e8c\u79cd\uff0c\u5728\u5176\u4e2d\u522e\u75d5\u8bd5\u4ef6\u7528\u4e8e\u68c0\u9a8c\u6f06\u5c42\u635f\u574f\u540e\u7684\u8010\u8150\u8680\u6027\uff0c\u8be6\u7ec6\u8bd5\u4ef6\u5219\u89c2\u67e5\u9540\u5c42\u7684\u51fa\u6ce1\u548c\u9508\u8680\u7b49\u72b6\u51b5\u3002<\/p>\n

\n

\u5149\u7535\u50ac\u5316\u8bd5\u9a8c\u8bd5\u4ef6\u4e3a10 mm\u00d710 mm\u00d73 mm\uff0c\u8bd5\u9a8c\u524d\u8981704\u7845\u80f6\u5bc6\u5c01\u6027\u5de5\u4f5c\u53f0\u9762\u4e4b\u5916\u7684\u91d1\u5c5e\u8868\u5c42\u3002\u5c06\u8bd5\u4ef6\u6ce1\u6d78\u57283.5wt%\u7684NaCl\u9971\u548c\u6eb6\u6db2\u4e2d\uff0c\u68c0\u6d4b\u8bd5\u4ef6\u6ce1\u6d78\u4e0d\u4e00\u6837\u6642\u95f4\u540e\u7684\u5f15\u8def\u7535\u4f4d\u5dee\uff08OCP\uff09\u548c\u7535\u5316\u5b66\u963b\u6297\u8c31\uff08EIS\uff09\u3002\u8bd5\u9a8c\u9009\u7528PARSTAT 2273\uff08\u5bbe\u5915\u6cd5\u5c3c\u4e9a\u5927\u5b66\uff09\u7535\u5316\u5b66\u5de5\u4f5c\u7ad9\u5f00\u5c55\u68c0\u6d4b\uff0c\u8bd5\u4ef6\u4e3a\u5de5\u4f5c\u4e2d\u7535\u7ea7\uff0c\u9971\u548c\u7518\u6c5e\u7535\u6781\u4e3a\u53c2\u6bd4\u7535\u6781\uff0c\u94c2\u94cc\u4e1d\u4e3a\u534f\u52a9\u7535\u7ea7\uff0c\u626b\u63cf\u4eea\u5de5\u4f5c\u9891\u7387\u6807\u51c6\u4e3a100 kHz\uff5e10 mHz\uff0c\u6570\u636e\u4fe1\u53f7\u5e45\u5ea6\u503c\u4e3a20 mV\uff0c\u9009\u7528ZsimpWin\u8f6f\u4ef6\u5bf9\u6d4b\u8bd5\u6570\u636e\u5f00\u5c55\u7ebf\u6027\u62df\u5408\u3002<\/p>\n

\u00a0 \u00a0<\/strong><\/p>\n

\n
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\n
2 \u7d50\u679c\u4e0e\u63a2\u8ba8<\/strong><\/section>\n<\/section>\n<\/section>\n<\/section>\n

\n

2.1 \u5916\u90e8\u7ecf\u6d4e\u5916\u8c8c\u7279\u70b9<\/strong><\/p>\n

\n

\u6839\u636eFE-SEM\u89c2\u67e5\u77f3\u58a8\u70ef\u7684\u5916\u90e8\u7ecf\u6d4e\u5916\u8c8c\u7279\u70b9\uff0c\u7d50\u679c\u5982\u4e0b\u56fe1\u6240\u663e\u793a\u3002\u7531\u56fe1\u53ef\u4ee5\u770b\u5f97\u51fa\uff0c\u77f3\u58a8\u70ef\u5448\u900f\u660e\u8584\u7eb1\u6253\u5377\u6837\u5b50\uff0c\u8fd9\u4e5f\u662f\u56e0\u4e3a\u77f3\u58a8\u70ef\u8868\u9762\u8f83\u9ad8\uff0c\u975e\u5e38\u5bb9\u6613\u56e0\u8868\u5c42\u6b63\u7535\u8377\u4e0d\u5e73\u8861\u800c\u5931\u8861\uff0c\u6bc1\u574f\u77f3\u58a8\u70ef\u81ea\u8eab\u7684\u8868\u9762\u6784\u9020\uff0c\u56e0\u800c\u5c55\u73b0\u51fa\u8936\u5b50\u5916\u8c8c\u7279\u70b9\uff1bFT\u9540\u5c42\u8868\u5c42\u6709\u5c0f\u578b\u5f88\u591a\u5b54\u773c\u53ca\u8936\u5b50\uff0c\u800c\u52a0\u4e0a\u9002\u5f53\u77f3\u58a8\u70ef\u540e\uff0c\u9540\u5c42\u8868\u5c42\u6574\u5e73\u5149\u6d01\uff0c\u65e0\u663e\u8457\u7f3a\u70b9\uff0c\u5f53\u77f3\u58a8\u70ef\u6210\u5206\u505a\u52300.15wt%\u65f6\uff0c\u9540\u5c42\u8868\u5c42\u53d1\u751f\u8f83\u591a\u95f4\u9699\u3001\u88c2\u75d5\u7b49\u7f3a\u70b9\uff0c\u4e14\u6709\u56e2\u5706\u5757\u53d1\u751f\u3002<\/p>\n

\n

\"1.jpg\"<\/p>\n

\n

\u77f3\u58a8\u70ef\u3001\u6c1f\u78b3\u55b7\u6d82\u9540\u5c42\u3001\u6c1f\u78b3\u55b7\u6d82\/\u77f3\u58a8\u70ef\u590d\u5408\u578b\u9540\u5c42\u7684\u7ea2\u5916\u5149\u8c31\u56fe\u5982\u4e0b\u56fe2 \u6240\u663e\u793a\u3002\u77f3\u58a8\u70ef\u57283461 cm-1\uff0c1641cm-1\uff0c1384 cm-1 \u4e0a\u6709\u663e\u8457\u7684\u7279\u70b9\u5cf0\uff0c\u5728\u5176\u4e2d3461 cm-1\u5904\u8f83\u5bbd\u6d88\u5316\u5438\u6536\u5cf0\u4e3a\u6c34\u5206\u548c\u672a\u5f7b\u5e95\u590d\u539f\u7684\u6c28\u57fa\u4e0e\u7fa7\u57fa\u4e2d\u7684-OH\u4f38\u7f29\u5f0f\u9707\u52a8\u5cf0\uff0c1641 cm-1\u5904\u4e3aC=C\u70c3\u57fa\u7684\u4f38\u7f29\u5f0f\u9707\u52a8\u5cf0\uff0c1384 cm-1\u6709C-OH\u7684\u4f38\u7f29\u5f0f\u9707\u52a8\u5cf0\uff0c\u8868\u660e\u6240\u8fd0\u7528\u7684\u77f3\u58a8\u70ef\u5e26\u6709-OH\u3001-COOH\u7b49\u5b98\u80fd\u56e2\u5f02\u6784\uff0c\u4e0e\u53c2\u8003\u6587\u732e\u4e2d\u77f3\u58a8\u70ef\u7684FT-IR\u5149\u8c31\u56fe\u4e00\u81f4\u3002\u9540\u5c42\u7ea2\u5916\u5149\u8c31\u4e2d\uff0c1222 cm-1 \u548c1160 cm-1 \u5904\u4e3aC-F \u952e\u6d88\u5316\u5438\u6536\u5cf0\uff0c\u52a0\u4e0a\u77f3\u58a8\u70ef\u540e\uff0c3461 cm-1\u5904\u7684-OH\u6d88\u5316\u5438\u6536\u5cf0\u51e0\u4e4e\u5f7b\u5e95\u6d88\u9000\uff0c\u8fd9\u4e5f\u662f\u73af\u6c27\u6811\u8102\u5e72\u56fa\u7684\u7d50\u679c\uff0c\u4e14\u56e0\u4e3a\u77f3\u58a8\u70ef\u754c\u9762\u7684\u5b98\u80fd\u56e2\u6210\u5206\u8f83\u5c11\uff0c\u5bf9\u6c1f\u78b3\u6811\u8102\u7684\u5316\u5b66\u7ed3\u6784\u5371\u5bb3\u5c0f\uff0c\u4e14\u77f3\u58a8\u70ef\u4e0e\u6c1f\u78b3\u55b7\u6d82\u5173\u952e\u4ee5\u7269\u7406\u5b66\u6df7\u548c\u7684\u65b9\u6cd5\u76f8\u5bb9\uff0c\u56e0\u800c\u9540\u5c42\u7ea2\u5916\u5149\u8c31\u65e0\u663e\u8457\u8f6c\u53d8\u3002<\/p>\n

\n

\"2.jpg\"<\/p>\n

\n

2.2 \u878d\u5408\u6297\u538b\u5f3a\u5ea6\u548c\u8868\u9762\u5f20\u529b<\/strong><\/p>\n

\n

\u590d\u5408\u578b\u9540\u5c42\u7684\u878d\u5408\u6297\u538b\u5f3a\u5ea6\u548c\u8868\u9762\u5f20\u529b\u68c0\u6d4b\u7d50\u679c\u5982\u4e0b\u56fe3\u6240\u663e\u793a\uff0c\u4f34\u968f\u7740\u77f3\u58a8\u70ef\u7684\u52a0\u4e0a\uff0c\u878d\u5408\u6297\u538b\u5f3a\u5ea6\u548c\u8868\u9762\u5f20\u529b\u5747\u4e3b\u8981\u8868\u73b0\u4e3a\u672c\u6269\u5927\u540e\u51cf\u5c11\u7684\u53d1\u5c55\u8d8b\u52bf\u3002<\/p>\n

\n

\"3.jpg\"<\/p>\n

\n

\u878d\u5408\u6297\u538b\u5f3a\u5ea6\u5728G \u6210\u5206\u4e3a0.05wt%\u65f6\u505a\u5230\u8f83\u5927\uff0812.47 MPa\uff09\uff0c\u5bf9\u6bd4\u6c1f\u78b3\u55b7\u6d82\u9540\u5c42\u589e\u5f3a\u4e8644.33%\uff0c\u8868\u9762\u5f20\u529b\u8f6c\u53d8\u8f83\u5c0f\uff0c\u753176.76\u00b0\u63d0\u5347\u523082.52\u00b0\uff0c\u590d\u5408\u578b\u9540\u5c42\u7684\u758f\u6c34\u6027\u9010\u6b65\u63d0\u9ad8\u3002\u8fd9\u4e5f\u662f\u56e0\u4e3aG\u5177\u5907\u758f\u6c34\u6027\uff0c\u4e14\u7247\u5c42\u904d\u5e03\u7684G\u53ef\u4ee5\u6dfb\u5145\u9540\u5c42\u7f3a\u70b9\uff0c\u6269\u5927\u9540\u5c42\u81f4\u76f8\u5bf9\u5bc6\u5ea6\uff0c\u63d0\u5347\u6d82\u819c\u7684\u758f\u6c34\u6027\uff1b\u4e14G\u5177\u5907\u5f88\u5927\u7684\u6bd4\u8868\u9762\uff0c\u80fd\u6269\u5927\u73af\u6c27\u6811\u8102\u4e0e\u57fa\u6750\u89e6\u78b0\u603b\u9762\u79ef\uff0c\u8fdb\u800c\u63d0\u5347\u4e0e\u57fa\u6750\u7684\u7ed3\u5408\u6027\u3002\u4f46G\u6210\u5206\u8fc7\u9ad8\u65f6\uff0c\u6613\u5728\u672c\u8eab\u56fa\u5c42\u76f8\u4e92\u4f5c\u7528\u529b\u4e0b\u56e2\u5706\uff0c\u9020\u6210\u9540\u5c42\u5167\u90e8\u7f3a\u70b9\u589e\u52a0\uff0c\u6bc1\u574f\u4e86\u9540\u5c42\u7684\u6784\u9020\u548c\u7279\u6027\uff0c\u51cf\u5c11\u4e86\u9540\u5c42\u7684\u8868\u9762\u5f20\u529b\u548c\u878d\u5408\u6297\u538b\u5f3a\u5ea6\u3002\u9488\u5bf9\u9540\u5c42\u6765\u8bb2\uff0c\u5438\u6c34\u6027\u4f7f\u6eb6\u6db2\u975e\u5e38\u5bb9\u6613\u6e7f\u6da6\u63a5\u89e6\u9762\u79ef\uff0c\u63d0\u5347\u4e86\u8150\u5316\u7269\u8d28\u6e17\u5165\u8fdb\u9540\u5c42\u7684\u673a\u9047\uff0c\u8868\u9762\u5f20\u529b\u7684\u6269\u5927\u8868\u660e\u9540\u5c42\u8868\u5c42\u758f\u6c34\u6027\u7684\u63d0\u5347\uff0c\u6709\u76ca\u4e8e\u51cf\u7f13\u6eb6\u6db2\u7684\u6e17\u5165\uff1b\u5f53\u6c34\u7b49\u6d78\u8680\u9971\u548c\u6eb6\u6db2\u6839\u636e\u8513\u5ef6\u6e17\u900f\u5230\u5230\u57fa\u6750\u8868\u5c42\u540e\uff0c\u6d78\u8680\u7269\u8d28\u7684\u6c89\u79ef\u8513\u5ef6\u4f7f\u9540\u5c42\u4ea7\u751f\u53d1\u76b1\u9f13\u5305\uff0c\u6269\u5f20\u7535\u5316\u5b66\u8150\u8680\u5730\u533a\uff0c\u800c\u8f83\u9ad8\u7684\u878d\u5408\u6297\u538b\u5f3a\u5ea6\u4f7f\u9971\u548c\u6eb6\u6db2\u8513\u5ef6\u8270\u96be\uff0c\u63d0\u5347\u4e86\u9540\u5c42\u7684\u6297\u6e17\u7b49\u7ea7\u6027\uff0c\u51cf\u5c11\u4e86\u6d78\u8680\u62d3\u5c55\u8303\u7574\uff0c\u4f7f\u672a\u6e17\u5165\u4e00\u90e8\u5206\u4ecd\u80fd\u906d\u53d7\u9540\u5c42\u7684\u7ef4\u62a4\uff0c\u56e0\u800c\u63d0\u5347\u6d82\u819c\u7684\u8868\u9762\u5f20\u529b\u548c\u878d\u5408\u6297\u538b\u5f3a\u5ea6\u6709\u76ca\u4e8e\u63d0\u9ad8\u9540\u5c42\u957f\u671f\u6027\u9632\u8150\u8680\u529f\u6548\u3002<\/p>\n

\n

2.3 \u6d78\u8680\u5b89\u5168\u9632\u62a4\u7279\u6027<\/strong><\/p>\n

\n

2.3.1 \u76d0\u96fe\u8bd5\u9a8c<\/strong><\/p>\n

\n

\u635f\u574f\u9540\u5c42\u4e2d\u6027\u5316\u76d0\u96fe\u8bd5\u9a8c165 h\u540e\u7684\u7d50\u679c\u5982\u4e0b\u56fe4\u6240\u663e\u793a\u3002FT\u3001FT-G1\u548cFT-G15\u590d\u5408\u578b\u9540\u5c42\u7834\u635f\u7684\u5730\u65b9\u6d78\u8680\u72b6\u51b5\u663e\u8457\u6bd4FT-G5\u9540\u5c42\u6bd4\u8f83\u4e25\u91cd\uff0c\u6d78\u8680\u7269\u8d28\u5728\u95f4\u9699\u5904\u5f88\u591a\u6c89\u79ef\u4e43\u81f3\u9020\u6210\u9540\u5c42\u8131\u79bb\uff0c\u4e14\u635f\u574f\u5730\u533a\u4e4b\u5916\u7684\u4e00\u90e8\u5206\u6709\u663e\u8457\u5438\u6e7f\u9f13\u5305\u72b6\u51b5\u3002FT-G1\u9540\u5c42\u7684\u9f13\u5305\u603b\u9762\u79ef\u8d85\u8fc7\u522b\u7684\u9540\u5c42\uff0c\u800cFT-G5\u4ec5\u4ea7\u751f\u8f7b\u5ea6\u6d78\u8680\u3002\u8fd9\u662f\u7531\u4e8eFT-G5\u9540\u5c42\u4e0e\u5e95\u6750\u91d1\u5c5e\u6750\u6599\u7684\u878d\u5408\u6297\u538b\u5f3a\u5ea6\u8f83\u9ad8\uff0c\u6297\u9971\u548c\u6eb6\u6db2\u8513\u5ef6\u6e17\u5165\u5de5\u4f5c\u80fd\u529b\u5f3a\uff0c\u63d0\u5347\u4e86\u635f\u574f\u9540\u5c42\u5728\u8010\u8150\u8680\u81ea\u7136\u73af\u5883\u4e2d\u7684\u8010\u8150\u8680\u6027\u80fd\u3002<\/p>\n

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\"4.jpg\"<\/p>\n

\n

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\n

\"5.jpg\"<\/p>\n

\n

2.3.2 \u9540\u5c42\u5f15\u8def\u7535\u4f4d\u5dee\u5256\u6790<\/strong><\/p>\n

\n

\u56fe6\u4e3a\u590d\u5408\u578b\u9540\u5c42\u5f15\u8def\u7535\u4f4d\u5dee\uff08OCP\uff09\u968f\u8bd5\u9a8c\u6642\u95f4\u8f6c\u53d8\u66f2\u7ebf\u56fe\uff0c\u53ef\u4ee5\u770b\u5f97\u51fa\uff0c\u5404\u9540\u5c42\u7ba1\u7406\u4f53\u7cfb\u7684OCP\u5747\u6301\u7eed\u51cf\u5c11\uff0c\u4ea7\u751f\u6d78\u8680\u7684\u53d1\u5c55\u8d8b\u52bf\u6301\u7eed\u6269\u5927\u3002\u5728\u9540\u5c42\u4e2d\u52a0\u4e0aG \u540e\uff0cFT-G1\u9540\u5c42OCP\u5728\u8bd5\u9a8c\u524d\u671f\u9ad8\u8fc7FT\u9540\u5c42\uff0c\u4f46\u8bd5\u9a8c\u5230288 h\u540e\u4e8c\u8005\u7684OCP\u76f8\u8d34\u8fd1\uff0c\u5728\u8bd5\u9a8c720 h\u540e\u51cf\u5c11\u5230-350 mV\u4e0a\u4e0b\uff0cFT-G5\u9540\u5c42OCP\u5728\u6ce1\u6d78\u524d\u671f\u9ad8\u8fc70 mV\uff0c\u63a5\u7740\u6301\u7eed\u964d\u4f4e\uff0c\u5728\u8bd5\u9a8c720 h\u540e\u7ef4\u6301\u5728-300mV\u4ee5\u4e0a\uff0c\u800c\u5f53G\u6210\u5206\u505a\u52300.15wt%\u65f6\uff0cOCP\u5728\u524d\u671f\u4e0eFT\u9540\u5c42\u76f8\u4eff\uff0c\u5728288 h\u540e\u5927\u5e45\u5ea6\u7684\u964d\u4f4e\uff0c\u6700\u540e\u964d\u4f4e\u5230-473 mV\uff0c\u6d78\u8680\u53d1\u5c55\u8d8b\u52bf\u63d0\u5347\uff0cOCP\u6548\u51c6\u7684FT-G5\u9540\u5c42\u7684\u6d78\u8680\u8d8b\u5411\u5c0f\u4e8e\u522b\u7684\u9540\u5c42\u3002<\/p>\n

\n

\"6.jpg\"<\/p>\n

\n

2.3.3 \u9540\u5c42\u7279\u6027\u963b\u6297\u8c31\u5206\u6790<\/strong><\/p>\n

\n

\u56fe7 \u4e3aFT \u9540\u5c42\u548cFT-G \u590d\u5408\u578b\u9540\u5c42\u57283.5wt%\u7684NaCl\u4e2d\u6ce1\u6d78\u4e0d\u4e00\u6837\u6642\u95f4\u7684EIS\u56fe\uff0c\u80fd\u591f\u770b\u89c1\uff0cFT\u9540\u5c42\u548cFT-G1\u9540\u5c42\u5728\u8bd5\u9a8c6~168 h\u73af\u8282\uff0cNyquist\u56fe\u5c55\u73b0\u7684\u534a\u5f84\u6301\u7eed\u51cf\u5c0f\u7684\u53cc\u5bb9\u6297\u5f27\u7279\u70b9\uff0c\u5177\u59072\u4e2a\u7a33\u6001\u503c\uff0c\u8fd9\u4e5f\u662f\u56e0\u4e3a\u9971\u548c\u6eb6\u6db2\u8fc5\u901f\u6e17\u5165\u9540\u5c42\/\u91d1\u5c5e\u6750\u6599\u9875\u9762\uff0c\u9540\u5c42\u7535\u963b\u5668\u6301\u7eed\u51cf\u5c11\uff0c\u91d1\u5c5e\u6750\u6599\u53d1\u751f\u6d78\u8680\uff1b\u4f34\u968f\u7740\u6ce1\u6d78\u6642\u95f4\u7684\u589e\u52a0\uff0c\u9540\u5c42\/\u91d1\u5c5e\u6750\u6599\u9875\u9762\u7684\u9508\u8680\u7269\u8d28\u6162\u6162\u6c89\u79ef\uff0c\u8513\u5ef6\u5168\u8fc7\u7a0b\u906d\u53d7\u963b\u788d\uff0c\u5728Nyquist\u56fe\u5185\u4e3b\u8981\u8868\u73b0\u4e3a\u4f4e\u9891\u7387\u533a\u53d1\u751fWar-burg\u8513\u5ef6\u5c3e\u3002\u56e0\u4e3aFT-G1\u590d\u5408\u578b\u9540\u5c42\u7684\u77f3\u58a8\u70ef\u6210\u5206\u8f83\u4f4e\uff0c\u5bf9\u6d82\u819c\u7684\u6d78\u8680\u5b89\u5168\u9632\u62a4\u6027\u80fd\u7684\u5371\u5bb3\u8f83\u5c0f\uff0c\u56e0\u800c\u4e0e\u7eaf\u6c1f\u78b3\u55b7\u6d82\u9540\u5c42\u4e3b\u8981\u8868\u73b0\u76f8\u4eff\u3002\u4f34\u968f\u7740\u77f3\u58a8\u70ef\u6210\u5206\u7684\u8fdb\u4e00\u6b65\u63d0\u5347\uff0c\u590d\u5408\u578b\u9540\u5c42\u7684\u8010\u8150\u8680\u6027\u660e\u663e\u589e\u5f3a\uff0cFT-G5\u9540\u5c42\u57286\uff5e288 h\u73af\u8282\u7684Nyquist\u56fe\u4e3b\u8981\u8868\u73b0\u4e3a\u5355\u5bb9\u6297\u5f27\u7279\u70b9\uff0c\u8868\u660e\u9971\u548c\u6eb6\u6db2\u5411\u9540\u5c42\u7684\u6e17\u5165\u906d\u53d7\u5f88\u5927\u7684\u963b\u62e6\uff0c\u9540\u5c42\u5177\u5907\u8f83\u597d\u7684\u4fdd\u62a4\u529f\u6548\uff0c\u63a5\u7740\u53d1\u751f\u7684\u53cc\u5bb9\u6297\u5f27\u8868\u660e\u9971\u548c\u6eb6\u6db2\u6162\u6162\u6e17\u5165\u9540\u5c42\u3002\u91d1\u5c5e\u8868\u5c42\u4ea7\u751f\u7684\u6d78\u8680\u5fae\u5145\u7535\u7535\u6c60\u4f7f\u57fa\u6750\u4ea7\u751f\u6d78\u8680\uff0c\u4f46\u9540\u5c42\u4ecd\u4fdd\u6301\u7740\u8be6\u7ec6\uff0c\u5177\u5907\u4e00\u5b9a\u5b89\u5168\u9632\u62a4\u529f\u6548\u3002<\/p>\n

\n

\"7.jpg\"<\/p>\n

\n

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\n

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\n

\"8.jpg\"<\/p>\n

\n

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